The extent to which method validation (step 5) is investigated will depend on the use of the end analysis; for example, a method required for quality control will require more validation than one ...

Therefore, these parameters must be considered during method development and verified during validation. Recovery. After determination of the action level, sample recovery is determined from a 10-in.

When spatial data are correlated, currently available data-driven smoothing parameter selection methods for nonparametric regression will often fail to provide useful results. The authors propose a ...